Thionyl Chloride → HCID 54019687, compound

HRID 1196427Notes

Reaction equation

HRID 1196427 reaction equation
[CH2:1]([O:11][C:12]1[CH:17]=[CH:16][CH:15]=[C:14]([C:18]2[CH:23]=[CH:22][CH:21]=[CH:20][CH:19]=2)[C:13]=1[C:24]([OH:26])=O)[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH3:10].O=S(Cl)[Cl:29]>>[CH2:1]([O:11][C:12]1[CH:17]=[CH:16][CH:15]=[C:14]([C:18]2[CH:23]=[CH:22][CH:21]=[CH:20][CH:19]=2)[C:13]=1[C:24]([Cl:29])=[O:26])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH3:10]

Participants

3

Reactant 2

HCID 24386Thionyl ChlorideHCID 19898360HCID 19898360, compound

Product 1

HCID 54019687HCID 54019687, compound

Procedure

20 ml of SOCl2 was added to 4 g (1.13×10-2 mol) of decyloxybiphenylcarboxylic acid, and the mixture was heated at reflux for 3.5 hours. Excessive SOCl2 was evaporated to obtain decyloxybiphenylcarboxylic acid chloride.

Workup

  1. temperaturethe mixture was heated
  2. temperatureat reflux for 3.5 hours
  3. customExcessive SOCl2 was evaporated

Sources & evidence

ORD record
ord-28bc16bc3a2c47169a326e4ed35f05e8
Source dataset
uspto-grants-1992_05
Patent number
US05114613

Reaction notes

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