HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethylparaben → p-Heptoxybenzoic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethylparaben | HCID 8434 | — |
| Reactant | 1-Bromoheptane | HCID 12369 | — |
| Product | p-Heptoxybenzoic acid | HCID 85154 | — |
Reaction Steps
Using ethyl p-hydroxybenzoate (33.3 g, 0.20 mol) and n-heptyl bromide (39.4 g, 0.22 mol), the reaction was carried out in the same manner as described in Example 21, (1), and then recrystallized from ethanol to give the title compound as a white microneedles; yield: 19.0 g (40.2%); mp 86.2°-90.3° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05114615 |
| Source dataset | uspto-grants-1992_05 |
| ORD ID | ord-95e5b1fdf99f46c5ba2cd1a4e097888e |
| Source note | uspto-grants-1992_05 |