HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethyl Sulfoxide → HCID 19898648, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethyl Sulfoxide | HCID 679 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Oxalyl chloride | HCID 65578 | — |
| Reactant | HCID 19898714 | HCID 19898714 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 19898648 | HCID 19898648 | — |
Reaction Steps
The above alcohol (723 mg) was oxidised under Swern conditions (dimethyl sulphoxide (450 mg), oxalyl chloride (248 μl), triethylamine (1.58 ml)) in dichloromethane (25 ml) to give 8-(2-quinolinyloxy)octan-1-al. This was used directly in the next stage.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05114940 |
| Source dataset | uspto-grants-1992_05 |
| ORD ID | ord-7c799f2bdc1d4d80b246f5b4fc93fa9d |
| Source note | uspto-grants-1992_05 |