HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethyl Sulfoxide → HCID 19898708, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethyl Sulfoxide | HCID 679 | — |
| Reactant | Oxalyl chloride | HCID 65578 | — |
| Reactant | HCID 19898683 | HCID 19898683 | — |
| Solvent | Triethylamine | HCID 8471 | — |
| Product | HCID 19898708 | HCID 19898708 | — |
Reaction Steps
The above alcohol was oxidised under Swern conditions (dimethyl sulphoxide, 0.615 g; oxalyl chloride, 0.38 ml; triethylamine, 2.74 ml) to give after column chromatography 11-(2-quinolinyloxy)undecan-2-one (0.96 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05114940 |
| Source dataset | uspto-grants-1992_05 |
| ORD ID | ord-a1109942865c44d3bd7b9fb74229bc19 |
| Source note | uspto-grants-1992_05 |