HuagongsheHuagongshe Chemistry Print Report · For research reference only
Piperidine → HCID 67853764, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Piperidine | HCID 8082 | — |
| Reactant | HCID 19786539 | HCID 19786539 | — |
| Product | HCID 67853764 | HCID 67853764 | — |
Reaction Steps
6,7-Dihydro-5-dimethylaminomethyl-3-phenyl-1,2-benzisoxazol-4(5H)-one hydrochloride (0.80 g) was warmed with 5 ml of piperidine (4.31 g) at 90° C. for 20 minutes. The excess piperidine was removed in vacuo and the hydrochloride was formed in ethereal HCl to give 0.95 g of 6,7-dihydro-5-(1-piperidinylmethyl)-3-phenyl-1,2-benzisoxazol-4(5H)-one hydrochloride hemihydrate, m.p. 182°-183° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05114936 |
| Source dataset | uspto-grants-1992_05 |
| ORD ID | ord-002accf16d794efeb722a86abdc9427c |
| Source note | uspto-grants-1992_05 |