Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Styrene | HCID 7501 | — |
| Reactant | Butyl Acrylate | HCID 8846 | — |
| Reactant | Potassium Persulfate | HCID 24412 | — |
| Solvent | Water | HCID 962 | — |
| Product | Butyl prop-2-enoate;styrene | HCID 168422 | — |
Reaction Steps
Water and octylphenylhydroxypolyoxyethylene were mixed in a glass reaction vessel fitted with a stirrer, and the mixture was heated to 70° C. Butyl acrylate, styrene and the crosslinking monomer were added, followed by potassium persulfate in aqueous solution. The resulting mixture was stirred at a rate of the order of 250 rpm, while the temperature was maintained at 70° C. The polymerization time was 4 hours. The resulting latex had a solid content of 22.8% by weight, and a mean particle diameter of 330 nm.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US05115031 |
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| Source dataset | uspto-grants-1992_05 |
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| ORD ID | ord-7e5f2b1e1a9a45ef91876ad4b326d555 |
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| Source note | uspto-grants-1992_05 |
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