Glycerol → HCID 15292827, compound

HRID 1196748Notes

Reaction equation

HRID 1196748 reaction equation
[O:1]=[CH:2][C:3]([Cl:6])([Cl:5])[Cl:4].S(=O)(=O)(O)O.[OH:12][CH2:13][CH:14]([CH2:16]O)[OH:15]>>[Cl:4][C:3]([Cl:6])([Cl:5])[CH:2]1[O:15][CH:14]([CH2:13][OH:12])[CH2:16][O:1]1

Participants

4

Reactant 3

HCID 753GlycerolHCID 1118Sulfuric AcidHCID 6407Chloral

Product 1

HCID 15292827HCID 15292827, compound

Procedure

A mixture of 16 g of chloral, 5 g of glycerine and 5 ml of concentrated sulphuric acid is,heated on a water-bath for 10 hours, then the reaction mixture is distilled in vacuo.

Workup

  1. distillationthe reaction mixture is distilled in vacuo

Sources & evidence

ORD record
ord-083c2c5456f44a7b9c2e4debc4c136d1
Source dataset
uspto-grants-1992_05
Patent number
US05116402

Reaction notes

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