HCID 15292827, compound → HCID 53897947, compound

HRID 1196754Notes

Reaction equation

HRID 1196754 reaction equation
[Cl:1][C:2](Cl)([Cl:10])[CH:3]1[O:7][CH:6]([CH2:8][OH:9])[CH2:5][O:4]1>[Zn].C(O)(=O)C>[Cl:1][CH:2]([Cl:10])[CH:3]1[O:7][CH:6]([CH2:8][OH:9])[CH2:5][O:4]1

Participants

4

Reactant 1

HCID 15292827HCID 15292827, compound

Product 1

HCID 53897947HCID 53897947, compound

Reagents, catalysts & solvents 2

HCID 23994ZincCatalystHCID 176Acetic AcidSolvent

Procedure

To a mixture of 5.5 g of 2-(trichloro-methyl)-4-(hydroxy-methyl)-dioxolan and 30 ml of acetic acid under stirring 1.6 g of zinc dust are added within 30 minutes. After a further 15 minutes of stirring the reaction mixture is distilled.

Workup

  1. additionare added within 30 minutes
  2. distillationis distilled

Sources & evidence

ORD record
ord-d281de7264364d28bf7671b6a884fdb5
Source dataset
uspto-grants-1992_05
Patent number
US05116402

Reaction notes

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