Chloral → Ethanol, 2,2,2-trichloro-1-(2-propenyloxy)-

HRID 1196755Notes

Reaction equation

HRID 1196755 reaction equation
[O:1]=[CH:2][C:3]([Cl:6])([Cl:5])[Cl:4].[CH2:7]([OH:10])[CH:8]=[CH2:9]>C1C=CC=CC=1>[Cl:4][C:3]([Cl:6])([Cl:5])[CH:2]([O:10][CH2:7][CH:8]=[CH2:9])[OH:1]

Participants

4

Reactant 2

HCID 6407ChloralHCID 7858Allyl Alcohol

Product 1

HCID 11095749Ethanol, 2,2,2-trichloro-1-(2-propenyloxy)-

Reagents, catalysts & solvents 1

HCID 241BenzeneSolvent

Procedure

A mixture of 7 g of chloral, 2.9 of allyl-alcohol and 15 ml of benzene is left standing for a night at room temperature, then distilled.

Workup

  1. waitis left
  2. waitstanding for a night at room temperature
  3. distillationdistilled

Sources & evidence

ORD record
ord-cef8f912923148c1830e50819cfc61c4
Source dataset
uspto-grants-1992_05
Patent number
US05116402

Reaction notes

Loading…