HRID1196756

反应详情

EQUATION

反应方程式

HRID 1196756 的结构方程式

PROCEDURE

实验过程

To a mixture of 5 g of vinyl acetate and 27 ml of ethanol acetone cooled on dry ice 5 g of dry chlorine gas are added, then it is left standing for a night at room temperature. The reaction is poured onto 50 g of ice-water. The product is extracted with 30 ml of chloroform, the extract is washed with a sodium hydrogen carbonate solution and water, then dried on magnesium sulfate and distilled.

WORKUP

后处理

  1. additionare added
  2. waitit is left
  3. waitstanding for a night at room temperature
  4. extractionThe product is extracted with 30 ml of chloroform
  5. washthe extract is washed with a sodium hydrogen carbonate solution and water
  6. customdried on magnesium sulfate
  7. distillationdistilled