HuagongsheHuagongshe Chemistry Print Report · For research reference only
Bromide ion → 2-Bromo-1,1-diethoxypropane
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Bromide ion | HCID 259 | — |
| Reactant | Propane, 1,1-diethoxy- | HCID 20858 | — |
| Solvent | Carbon Tetrachloride | HCID 5943 | — |
| Product | 2-Bromo-1,1-diethoxypropane | HCID 103001 | — |
Reaction Steps
13.22 g of propion-aldehyde-diethyl-acetal are dissolved in 15 ml of carbon tetrachloride; at -10° C. 20 ml of the carbon tetrachloride solution of 17.58 g of bromide are dropped to it under stirring. After its warming to room temperature it is distilled in vacuo.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05116402 |
| Source dataset | uspto-grants-1992_05 |
| ORD ID | ord-0eb4831cd9d74c588e59ab30b8a74767 |
| Source note | uspto-grants-1992_05 |