1-Methylheptyl 4-Benzyloxybenzoate → 4-(1-Methylheptyloxycarbonyl)phenol

HRID 1196793Notes

Reaction equation

HRID 1196793 reaction equation
C([O:8][C:9]1[CH:25]=[CH:24][C:12]([C:13]([O:15][CH:16]([CH3:23])[CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH3:22])=[O:14])=[CH:11][CH:10]=1)C1C=CC=CC=1.[H][H]>C(O)C.[Pd]>[OH:8][C:9]1[CH:25]=[CH:24][C:12]([C:13]([O:15][CH:16]([CH3:23])[CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH3:22])=[O:14])=[CH:11][CH:10]=1

Participants

5

Reactant 2

HCID 198881221-Methylheptyl 4-BenzyloxybenzoateHCID 178418361HCID 178418361, compound

Product 1

HCID 110103794-(1-Methylheptyloxycarbonyl)phenol

Reagents, catalysts & solvents 2

HCID 23938PalladiumCatalystHCID 702EthanolSolvent

Procedure

The compound obtained in (1) above was dissolved in 15 ml of ethanol, and 0.36 g of 10 % palladium-on-carbon was added to the solution to conduct hydrogenation in a hydrogen atmosphere to obtain 1.29 g of the titled compound.

Sources & evidence

ORD record
ord-652ddae31e90425c84bd712255a8bdb2
Source dataset
uspto-grants-1992_05
Patent number
US05116531

Reaction notes

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