HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1196804Generated: October 27, 2026
Thionyl Chloride → 5-Dodecylthiophene-2-carboxylic chloride
https://huagongshe.com/reaction/1196804
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 5-Dodecylthiophene-2-carboxylic acid | HCID 14985090 | — |
| Product | 5-Dodecylthiophene-2-carboxylic chloride | HCID 14985091 | — |
Reaction Steps
4 ml of thionyl chloride was added to 0.57 g (1.93×10-3 ml) of 5-dodecylthiophene-2-carboxylic acid, followed by heat-stirring for 4 hours at 70° C. and removal of excessive thionyl chloride by reduced-pressure distillation to obtain 5-dodecylthiophene-2-carboxylic chloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US05116530 |
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| Source dataset | uspto-grants-1992_05 |
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| ORD ID | ord-454ff0b992554db09d451386b47c9162 |
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| Source note | uspto-grants-1992_05 |
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