Ethyl 4-bromobutyrate → HCID 54556138, compound

HRID 1196819Notes

Reaction equation

HRID 1196819 reaction equation
Br[CH2:2][CH2:3][CH2:4][C:5]([O:7]CC)=O.[CH3:10][CH:11]([CH2:14][CH2:15][CH2:16][CH3:17])[CH:12]=O>>[CH3:10][CH:11]([CH2:14][CH2:15][CH2:16][CH3:17])[CH:12]=[CH:2][CH2:3][CH2:4][CH2:5][OH:7]

Participants

3

Reactant 2

HCID 76300Ethyl 4-bromobutyrateHCID 1025152-Methylhexanal

Product 1

HCID 54556138HCID 54556138, compoundYield 52%

Procedure

6-methyl-4-decen-1-ol was prepared in the same manner according to Example 4 except that 97.5 g (0.5 mol) of ethyl 4-bromobutyrate was used in place of ethyl 5-bromovalerate and 57.1 g (0.5 mol) of 2-methyl hexanal was used in place of 2-methyl valeraldehyde.

Sources & evidence

ORD record
ord-27c6c1e5634646908180b926d0b73256
Source dataset
uspto-grants-1992_05
Patent number
US05116813

Reaction notes

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