3-Methylbutanal → HCID 53780734, compound

HRID 1196820Notes

Reaction equation

HRID 1196820 reaction equation
Br[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][C:7]([O:9]CC)=O.[CH:12](=O)[CH2:13][CH:14]([CH3:16])[CH3:15]>>[CH3:15][CH:14]([CH3:16])[CH2:13][CH:12]=[CH:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][OH:9]

Participants

3

Reactant 2

HCID 115523-MethylbutanalHCID 117544Ethyl 6-bromohexanoate

Product 1

HCID 53780734HCID 53780734, compoundYield 50%

Procedure

9-methyl-6-decen-1-ol was prepared in the same manner according to Example 4 except that 111.56 g (0.5 mol) of ethyl 6-bromohexanoate was used in place of ethyl 5-bromovalerate and 43.07 g (0.5 mol) of isovaleraldehyde was used in place of 2-methyl valeraldehyde.

Sources & evidence

ORD record
ord-c8a237eeccf9408dab93b43cf00e2c73
Source dataset
uspto-grants-1992_05
Patent number
US05116813

Reaction notes

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