HuagongsheHuagongshe Chemistry Print Report · For research reference only
Lithium Hydroxide → HCID 14724812, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Lithium Hydroxide | HCID 3939 | — |
| Reactant | Sodium Bisulfate | HCID 516919 | — |
| Reactant | HCID 14724810 | HCID 14724810 | — |
| Solvent | Water | HCID 962 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 14724812 | HCID 14724812 | — |
Reaction Steps
20.1 g (0.053 mol) of Boc-Phe-Nva-OMe (Example 1a) are suspended in 30 ml of water and 30 ml of dioxane. 2.5 g (0.106 mol) of lithium hydroxide are introduced at room temperature, and the mixture is stirred at room temperature for 3 hours. The reaction solution is acidified with 10% strength sodium bisulfate solution, and the product is filtered off with suction and stirred with diisopropyl ether.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05116835 |
| Source dataset | uspto-grants-1992_05 |
| ORD ID | ord-366682f3fd5f4e14b16d8613e7c1db41 |
| Source note | uspto-grants-1992_05 |