HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,5-Dibromopentane → N-[5-(Dimethylamino)pentyl]-3-phenyl-N-[2-[(phenylmethyl)thio]phenyl]-2-propenamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,5-Dibromopentane | HCID 8100 | — |
| Reactant | 3-Phenylprop-2-enoyl chloride | HCID 66023 | — |
| Reactant | 2-(Benzylthio)aniline | HCID 80616 | — |
| Reactant | HCID 19896890 | HCID 19896890 | — |
| Product | N-[5-(Dimethylamino)pentyl]-3-phenyl-N-[2-[(phenylmethyl)thio]phenyl]-2-propenamide | HCID 54307346 | — |
Reaction Steps
Following the method described in Example 5 but substituting the product of the reaction of 2-(benzylthio)aniline and cinnamoyl chloride for the 2-(benzylthio)phenylacetanilide and using 1,5-dibromopentane in place of 1,4-dibromobutane, the title compound is obtained. This material was isolated as a pale yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05116851 |
| Source dataset | uspto-grants-1992_05 |
| ORD ID | ord-2b3400f1ae9f425ba62aa5ae032b800c |
| Source note | uspto-grants-1992_05 |