HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetaldehyde → HCID 14127108, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetaldehyde | HCID 177 | — |
| Reactant | Thiophene | HCID 8030 | — |
| Reactant | Benzamide, 4-(1-methylethyl)- | HCID 69277 | — |
| Solvent | Acetic acid sulfuric acid | HCID 23350293 | — |
| Product | HCID 14127108 | HCID 14127108 | 5% |
Reaction Steps
Thiophene (25 mmol), acetaldehyde (20 mmol) and 4-isopropylbenzamide (10 mmol) were stirred in a mixture of acetic acid/sulfuric acid (10 ml/0.2 ml) at 60° C. for one hour to obtain N-[1-(2-thienyl)ethyl]-4-isopropylbenzamide. Yield: 5%. A large part of the product was a tar-like material.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05117000 |
| Source dataset | uspto-grants-1992_05 |
| ORD ID | ord-22e6f5daa7624279bcaab12778e7c1e6 |
| Source note | uspto-grants-1992_05 |