Acetaldehyde → HCID 14127108, compound

HRID 1197153Notes

Reaction equation

HRID 1197153 reaction equation
[S:1]1[CH:5]=[CH:4][CH:3]=[CH:2]1.[CH:6](=O)[CH3:7].[CH:9]([C:12]1[CH:20]=[CH:19][C:15]([C:16]([NH2:18])=[O:17])=[CH:14][CH:13]=1)([CH3:11])[CH3:10]>C(O)(=O)C>[S:1]1[CH:5]=[CH:4][CH:3]=[C:2]1[CH:6]([NH:18][C:16](=[O:17])[C:15]1[CH:19]=[CH:20][C:12]([CH:9]([CH3:11])[CH3:10])=[CH:13][CH:14]=1)[CH3:7]

Participants

5

Procedure

Thiophene, acetaldehyde and 4-isopropylbenzamide were stirred in a mixture of acetic acid/concentrated hydrochloric acid in the following ratio under the following reaction condition to obtain N-[1-(2-thienyl)ethyl]-4-isopropylbenzamide. In Runs 1 and 2, a large part of the product was a tar-like material.

Sources & evidence

ORD record
ord-92c9f4fc81e3445b94eeb0ff60e8a75e
Source dataset
uspto-grants-1992_05
Patent number
US05117000

Reaction notes

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