HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trityl chloride → HCID 19897834, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trityl chloride | HCID 6456 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | HCID 22138552 | HCID 22138552 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 19897834 | HCID 19897834 | 85% |
Reaction Steps
50 mmol of 1a was treated for 12 hours with 60 mmol of trityl chloride and 120 mmol of triethylamine in 150 ml of boiling toluene. After conventional working up, the remaining oil was chromatographed (Flash chromatography, eluent chloroform) and gave 2a (yield 85%) m.p. 45° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05116992 |
| Source dataset | uspto-grants-1992_05 |
| ORD ID | ord-027c19c1c2ad4fca9793e7707a3e54d9 |
| Source note | uspto-grants-1992_05 |