Silver Nitrate → HCID 19897943, compound

HRID 1197200Notes

Reaction equation

HRID 1197200 reaction equation
[N+]([O-])([O-])=O.[Ag+:5].[CH3:6][C:7]([CH3:17])([CH2:11][CH:12]([CH2:15][CH3:16])[CH2:13][CH3:14])[C:8]([O-:10])=[O:9].[Na+]>>[CH3:17][C:7]([CH3:6])([CH2:11][CH:12]([CH2:13][CH3:14])[CH2:15][CH3:16])[C:8]([O-:10])=[O:9].[Ag+:5]

Participants

3

Reactant 2

HCID 24470Silver NitrateHCID 23687946HCID 23687946, compound

Product 1

HCID 19897943HCID 19897943, compound

Procedure

A solution of silver nitrate (2.12 g, 12.5 mmol. in 10 ml. of water) was added to a solution of sodium 2,2-dimethyl-4-ethylhexanoate (prepared in situ by mixing 2.5 ml. of 5N NaOH and 2.15 g of 2,2-dimethyl-4-ethylhexanoic acid in 30 ml. of water). A white precipitate formed immediately. The mixture was left stirring at room temperature for one hour (protected from light) which was separated out by filtration, washed repeatedly with water and dried under vacuum. Yield (90%).

Workup

  1. customA white precipitate formed immediately
  2. waitThe mixture was left
  3. customwas separated out by filtration
  4. washwashed repeatedly with water
  5. customdried under vacuum
  6. customYield (90%)

Sources & evidence

ORD record
ord-5a1fa239d79247aea215b13d07cfea0c
Source dataset
uspto-grants-1992_05
Patent number
US05117022

Reaction notes

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