Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Thionyl Chloride → 1,2,2-Trichloro-3,3-dimethylcyclopropanecarboxylic acid chloride
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Thionyl Chloride | HCID 24386 | — |
| 반응물 | 1,2,2-Trichloro-3,3-dimethylcyclopropanecarboxylic acid | HCID 13654696 | — |
| 생성물 | 1,2,2-Trichloro-3,3-dimethylcyclopropanecarboxylic acid chloride | HCID 13654698 | — |
반응 단계
The 1,2,2-trichloro-2,2-dimethylcyclopropanecarboxylic acid (3.0 g) synthesized in Example k and thionyl chloride (1.0 ml) were mixed, and reacted at 60° C. The reaction mixture was distilled under reduced pressure to give the desired 1,2,2-trichloro-3,3-dimethylcyclopropanecarboxylic acid chloride (2.8 g) represented by the following formula. ##STR26##
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05117053 |
| 출처 데이터셋 | uspto-grants-1992_05 |
| ORD ID | ord-a5e1e5dab19f4cd7beff91b9fcff59c2 |
| 출처 메모 | uspto-grants-1992_05 |