HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl 6-benzoyloxyhexanoate → 6-(Benzoyloxy)hexanoic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl 6-benzoyloxyhexanoate | HCID 15222233 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | 6-(Benzoyloxy)hexanoic acid | HCID 15222234 | — |
Reaction Steps
To a solution of benzyl 6-benzoyloxy-hexanoate (c) (38.09 g) in ethyl acetate was added 5% Pd/C (3 g) and the resultant mixture was stirred under a hydrogen atmosphere for 24 hours. The crude product obtained by treating in the conventional manner was distilled under reduced pressure (1 mmHg, 182°-192° C.) to give the title compound (d). Yield: 4.92 g (90%)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05117042 |
| Source dataset | uspto-grants-1992_05 |
| ORD ID | ord-a9f1c3d47b274311a24c908f47d80420 |
| Source note | uspto-grants-1992_05 |