HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzoyl chloride → N'-t-butyl-N-(2-hydroxymethylbenzoyl)-N'-benzoylhydrazine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzoyl chloride | HCID 7412 | — |
| Reactant | N'-t-butyl-N-(2-hydroxymethylbenzoyl)hydrazine | HCID 19368051 | — |
| Solvent | Sodium Hydroxide | HCID 14798 | — |
| Product | N'-t-butyl-N-(2-hydroxymethylbenzoyl)-N'-benzoylhydrazine | HCID 19367869 | 58.4% |
Reaction Steps
0.7 g of N'-t-butyl-N-(2-hydroxymethylbenzoyl)-hydrazine and 1.1 g benzoyl chloride are combined in 10 ml of 5% NaOH and stirred at room temperature for 1.5 hours. The solids are filtered off, washed with water, then ether, to afford 0.6 g of white solid N'-t-butyl-N-(2-(benzoyloxymethyl)benzoyl)-N'-benzoylhydrazine. m.p. 190°-191° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05117057 |
| Source dataset | uspto-grants-1992_05 |
| ORD ID | ord-104e7490d8f14a38b087ec033a8d6352 |
| Source note | uspto-grants-1992_05 |