HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → N'-t-butyl-N-(3-toluoyl)-N'-benzoylhydrazine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | 3-Methylbenzoyl chloride | HCID 74375 | — |
| Reactant | N-(tert-butyl)benzohydrazide | HCID 1275961 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | N'-t-butyl-N-(3-toluoyl)-N'-benzoylhydrazine | HCID 15294604 | — |
Reaction Steps
To a stirred mixture of N'-t-butyl-N'-benzoylhydrazine (1.0 g) in 15 ml toluene and aqueous sodium hydroxide (0.5 g of 50% NaOH) was added 3-toluoylchloride (0.9 g). After stirring for 2 hours, the product was isolated by filtration to give N'-t-butyl-N-(3-toluoyl)-N'-benzoylhydrazine in good yield. m.p. 111°-114° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05117057 |
| Source dataset | uspto-grants-1992_05 |
| ORD ID | ord-23c4544bf15149a5b6ef32a1166e3efc |
| Source note | uspto-grants-1992_05 |