Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | 4-(Chloromethyl)pyridinium chloride | HCID 74570 | — |
| Reactant | N-(tert-butyl)benzohydrazide | HCID 1275961 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 15767549 | HCID 15767549 | — |
Reaction Steps
A solution of N'-t-butyl-N'-benzoylhydrazine (0.5 g, 0.00026 mol) in 10 ml of toluene was treated with 50% sodium hydroxide (0.6 g) followed by isonicotinyl chloride hydrochloride (0.47 g, 0.0026 mol). The mixture was stirred at 23° C. overnight. The solids were removed by filtration and washed with isonicotinyl-N'-benzoylhydrazine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US05117057 |
|---|
| Source dataset | uspto-grants-1992_05 |
|---|
| ORD ID | ord-071156054204481cb784d2b8e5a20d8b |
|---|
| Source note | uspto-grants-1992_05 |
|---|
