Benzoyl chloride → HCID 15452004, compound

HRID 1197283Notes

Reaction equation

HRID 1197283 reaction equation
[C:1]([NH:5][NH:6][C:7]([C:9]1[O:10][CH:11]=[CH:12][CH:13]=1)=[O:8])([CH3:4])([CH3:3])[CH3:2].[OH-].[Na+].[C:16](Cl)(=[O:23])[C:17]1[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=1>C1(C)C=CC=CC=1.O>[C:1]([N:5]([C:16](=[O:23])[C:17]1[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=1)[NH:6][C:7]([C:9]1[O:10][CH:11]=[CH:12][CH:13]=1)=[O:8])([CH3:4])([CH3:2])[CH3:3]

Participants

6

Reactant 3

HCID 7412Benzoyl chlorideHCID 14798Sodium HydroxideHCID 15452036HCID 15452036, compound

Product 1

HCID 15452004HCID 15452004, compound

Reagents, catalysts & solvents 2

HCID 962WaterSolventHCID 1140TolueneSolvent

Procedure

N'-t-butyl-N-(2-furoyl)hydrazine (1.0 g) was dissolved in 10 ml toluene and 2 ml water. 50% aqueous sodium hydroxide (1.0 g) was added followed by benzoylchloride (0.8 g). After stirring for 14 hours at room temperature, the solid product, N'-t-butyl-N-(2-furoyl)-N'-benzoylhydrazine, was removed by filtration and washed with water. m.p. 160°-162° C.

Workup

  1. customthe solid product, N'-t-butyl-N-(2-furoyl)-N'-benzoylhydrazine, was removed by filtration
  2. washwashed with water

Sources & evidence

ORD record
ord-269e8789739b452b918ee0e3970bcc1e
Source dataset
uspto-grants-1992_05
Patent number
US05117057

Reaction notes

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