HuagongsheHuagongshe Chemistry Print Report · For research reference only
N'-t-butyl-N'-(3-methylbenzoyl)hydrazine → N'-t-butyl-N-(2-phenyl-3-methylpentanoyl)-N'-(3-toluoyl)hydrazine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N'-t-butyl-N'-(3-methylbenzoyl)hydrazine | HCID 15452040 | — |
| Reactant | 3-Methyl-2-phenylvaleryl chloride | HCID 21886026 | — |
| Catalyst | Sodium Hydroxide | HCID 14798 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | N'-t-butyl-N-(2-phenyl-3-methylpentanoyl)-N'-(3-toluoyl)hydrazine | HCID 15452019 | — |
Reaction Steps
To a stirred suspension of N'-t-butyl-N'-(3toluoyl)hydrazine (0.7 g) in toluene (10 ml) and aqueous sodium hydroxide (12 drops of 50% aqueous sodium hydroxide) was added dropwise 2-phenyl-3-methyl-pentanoyl chloride (1.0 g). The reaction mixture was stirred overnight, diluted with hexanes and the solids filtered. The solids were washed with hexane and air dried.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05117057 |
| Source dataset | uspto-grants-1992_05 |
| ORD ID | ord-42a113d0cf8b4d84ba61a9873e270a79 |
| Source note | uspto-grants-1992_05 |