2-Propyl-2-oxetanemethanol → 1-(7-Methoxyhept-5-ynyl)-4-n-propyl-2,6,7-trioxabicyclo[2.2.2]octane

HRID 1197355Notes

Reaction equation

HRID 1197355 reaction equation
[CH3:1][O:2][CH2:3][C:4]#[C:5][CH2:6][CH2:7][CH2:8][CH2:9][C:10]([OH:12])=[O:11].[OH:13][CH2:14][C:15]1([CH2:19][CH2:20][CH3:21])[CH2:18]O[CH2:16]1>>[CH3:1][O:2][CH2:3][C:4]#[C:5][CH2:6][CH2:7][CH2:8][CH2:9][C:10]12[O:13][CH2:14][C:15]([CH2:19][CH2:20][CH3:21])([CH2:18][O:12]1)[CH2:16][O:11]2

Participants

3

Reactant 2

HCID 1838902-Propyl-2-oxetanemethanolHCID 19373304HCID 19373304, compound

Product 1

HCID 193733241-(7-Methoxyhept-5-ynyl)-4-n-propyl-2,6,7-trioxabicyclo[2.2.2]octane

Procedure

1-(7-Methoxyhept-5-ynyl)-4-n-propyl-2,6,7-trioxabicyclo[2.2.2]octane was prepared from 8-methoxyoct-6-ynoic acid and 3-hydroxymethyl-3-n-propyloxetane using the methodology described in Example 1.

Sources & evidence

ORD record
ord-5d2748d3368740a591f34185282287ae
Source dataset
uspto-grants-1992_05
Patent number
US05116862

Reaction notes

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