HuagongsheHuagongshe Chemistry Print Report · For research reference only
(2S,3R,4S)-2-[(tert-Butyloxycarbonyl)amino]-1-cyclohexyl-3,4-dihydroxy-6-methylheptane → HCID 4710, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (2S,3R,4S)-2-[(tert-Butyloxycarbonyl)amino]-1-cyclohexyl-3,4-dihydroxy-6-methylheptane | HCID 9974740 | — |
| Solvent | Hydrochloric Acid | HCID 313 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 4710 | HCID 4710 | — |
Reaction Steps
(2S,3R,4S)-2-[(tert-Butyloxycarbonyl)amino]-1-cyclohexyl-3,4-dihydroxy-6-methylheptane (5.05 g, 14.7 mmol, Luly et al., J. Org. Chem. 1988, 53, 6109) was stirred for 90 min in 4M hydrochloric acid in ethanol and then evaporated. Ether was added and evaporated 3 times and the residue was dried under high vacuum. The title compound was used without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05275950 |
| Source dataset | uspto-grants-1994_01 |
| ORD ID | ord-33aa4ab8a4134d38bc684a4195ba88d2 |
| Source note | uspto-grants-1994_01 |