HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 15657628, compound → HCID 15657635, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 15657628 | HCID 15657628 | — |
| Reactant | Potassium trimethylsilanolate | HCID 23668039 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 15657635 | HCID 15657635 | 60% |
Reaction Steps
A solution of the compound from Example 41 (15.5 g, 71.7 mmol) and potassium trimethylsilanolate (17.4 g) in 100 ml of THF was refluxed for 24 hours. After workup the title compound (8.7 g, 52%) was obtained as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05276053 |
| Source dataset | uspto-grants-1994_01 |
| ORD ID | ord-7613fded6bb44a86b46d0ea624991df5 |
| Source note | uspto-grants-1994_01 |