HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tetrahydrofuran → HCID 67820647, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tetrahydrofuran | HCID 8028 | — |
| Reactant | HCID 15657643 | HCID 15657643 | — |
| Reactant | Potassium trimethylsilanolate | HCID 23668039 | — |
| Product | HCID 67820647 | HCID 67820647 | — |
Reaction Steps
A solution of the compound from Example 16 (4.4 g, 17 mmol) and potassium trimethylsilanolate (4.36 g, 34 mmol) in 50 ml THF was refluxed for 2 hours. The precipitate was collected by filtration, dissolved in water and acidified with 1N HCl. After further workup, the title compound was obtained as a white solid (3.9 g, 99%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05276053 |
| Source dataset | uspto-grants-1994_01 |
| ORD ID | ord-610e625cfdec46b28e8b491b736c1809 |
| Source note | uspto-grants-1994_01 |