Methanol → HCID 131717093, compound

HRID 1197540Notes

Reaction equation

HRID 1197540 reaction equation
[N:1]([C:4]12[CH2:13][CH2:12][CH2:11][CH2:10][CH:9]1[CH2:8][O:7][C:6]1[CH:14]=[CH:15][CH:16]=[CH:17][C:5]2=1)=[C:2]=[O:3].[CH3:18][OH:19]>>[CH3:18][O:19][C:2](=[O:3])[NH:1][C:4]12[CH2:13][CH2:12][CH2:11][CH2:10][CH:9]1[CH2:8][O:7][C:6]1[CH:14]=[CH:15][CH:16]=[CH:17][C:5]2=1

Participants

3

Reactant 2

HCID 887MethanolHCID 19107030HCID 19107030, compound

Product 1

HCID 131717093HCID 131717093, compound

Procedure

A solution of the product from Example 71 (0.66 g, 2.88 mmol) in 20 ml methanol was refluxed 18 hours. Evaporation and chromatography gave the title compound (0.75 g).

Workup

  1. customEvaporation and chromatography

Sources & evidence

ORD record
ord-7f37e7fda75f45bfae67982c0cce9776
Source dataset
uspto-grants-1994_01
Patent number
US05276053

Reaction notes

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