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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1197568Generated: November 1, 2026

N-methyl-2-pyrrolidone → HCID 53723146, compound

https://huagongshe.com/reaction/1197568

Reaction equation

Participants

RoleNameHCIDCharge
ReactantN-methyl-2-pyrrolidoneHCID 13387—
ReactantSodium hydrideHCID 24758—
ReactantHCID 67850672HCID 67850672—
CatalystCopperHCID 23978—
ProductHCID 53723146HCID 53723146—

Reaction Steps

2-(4-cyano-phenyl)-5-[4-(2-methoxycarbonyl-ethyl)-phenyl]-3,4-dihydro-2H,5H-1,2,5-thiadiazole-1,1-dioxide 4-Fluoro-benzonitrile and sodium hydride in N-methyl-pyrrolidone were used without copper salts.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05276049
Source datasetuspto-grants-1994_01
ORD IDord-369fa61ae6c3400ea435174cf1f40dfc
Source noteuspto-grants-1994_01