Vinyltrimethoxysilane → HCID 19107180, compound

Participants

Reaction Conditions

Reaction Steps

A mixture of the 20.67 g (68.1 mmol) of 1-(3-(2,2,4-trimethyl-1-aza-2-silacyclopentyl)propyl-1,1,3,3-tetramethyldisiloxane, 10.6 g (71.5 mmol) of vinyltrimethoxysilane which had been distilled from sodium, and 0.03 g of a chloroplatinic acid-1,3-divinyl-1,1,3,3-tetramethyldisiloxane complex having about 0.7 weight percent platinum was heated for one hour at 120° C. The resulting product was distilled and the distillate was collected at 152° C. and 0.1 mm Hg. The amount of distillate collected was 28.2 g of 1-(3-(2,2,4-trimethyl-1-aza-2-silacyclopentyl)propyl)-3-(2-trimethoxysilylethyl)-1,1,3,3-tetramethyldisiloxane which was identified by 13C and 29Si NMR (nuclear magnetic resonance) and GC-MS.

Provenance & Evidence