Acetic Acid → HCID 19107423, compound

Participants

Reaction Steps

5.40 g (100 mmol) of sodium methoxide was dissolved in 40 ml of anhydrous methanol. To this solution was added, with ice-cooled, 4.04 g (10 mmol) of 1,4-dihydro-2,6-dimethyl-4-(3-nitrophenyl)-3-pyridylpyridine-3-carboxylate. The reaction mixture was stirred for 5 hours and neutralized with acetic acid. To this reaction mixture was added 400 ml of water. Crystals separated were collected, washed with water and dried under reduced pressure, whereby the captioned compound was obtained. The yield was 2.45 g (70%).

Provenance & Evidence