HuagongsheHuagongshe Chemistry Print Report · For research reference only
Maleic Anhydride → HCID 86748798, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Maleic Anhydride | HCID 7923 | — |
| Reactant | N-Methylsuccinimide | HCID 70717 | — |
| Catalyst | Nickel | HCID 935 | — |
| Catalyst | HCID 131718302 | HCID 131718302 | — |
| Solvent | N-methyl-2-pyrrolidone | HCID 13387 | — |
| Product | HCID 86748798 | HCID 86748798 | 44% |
Reaction Steps
U.S. Application No. 4,731,454 describes the preparation of N-methylpyrrolidone (NMP) by hydrogenating N-methylsuccinimide on a cobalt/rhenium/molybdenum catalyst. U.S. Application No. 3,109,005 discloses a process for the preparation of NMP by hydrogenating maleic anhydride (MAA)/methylamine mixtures on a Raney nickel catalyst. At reaction times of 10 hours, NMP yields of 70% are achieved in this process. According to the process of DE-A 22 00 600, NMP is obtained in a yield of 44% under the most favorable conditions by hydrogenating MAA/methylamine mixtures on palladium supported catalysts.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05276165 |
| Source dataset | uspto-grants-1994_01 |
| ORD ID | ord-864df0a815a141f6a64297e0c932249b |
| Source note | uspto-grants-1994_01 |