HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 67657348, compound → HCID 53940374, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 67657348 | HCID 67657348 | — |
| Reactant | Butyllithium | HCID 178418339 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Solvent | Hexane | HCID 8058 | — |
| Product | HCID 53940374 | HCID 53940374 | — |
Reaction Steps
The tosylhydrazone (20) in tetrahydrofuran is treated with n-butyl lithium (BuLi, b) in hexane and the mixture is stirred at room temperature for 16 hours. Aqueous work up is followed by extraction and purification to yield the diene (21).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05278141 |
| Source dataset | uspto-grants-1994_01 |
| ORD ID | ord-26f761ea17f2494a831cecccec7fcd10 |
| Source note | uspto-grants-1994_01 |