HuagongsheHuagongshe Chemistry Print Report · For research reference only
Toluene → Phosphonium, (8-carboxyoctyl)triphenyl-, bromide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Toluene | HCID 1140 | — |
| Reactant | Triphenylphosphine | HCID 11776 | — |
| Reactant | 8-Bromooctanoic acid | HCID 548275 | — |
| Product | Phosphonium, (8-carboxyoctyl)triphenyl-, bromide | HCID 10918084 | — |
Reaction Steps
Dissolve 8-bromooctanoic acid (1.0g) in anhydrous toluene (3 mL) and add triphenylphosphine (1.21g). Heat to reflux overnight. Separate the lower phase crystallize (ethanol/ethyl ether) to give (8-carboxyoctyl)triphenylphosphonium bromide (1.0g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05278171 |
| Source dataset | uspto-grants-1994_01 |
| ORD ID | ord-d71a91073f9f47eaa40aea6e64d9b062 |
| Source note | uspto-grants-1994_01 |