HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 53672027, compound → 12,12,12-trifluorododecanoic Acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 53672027 | HCID 53672027 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 12,12,12-trifluorododecanoic Acid | HCID 9813738 | — |
Reaction Steps
Dissolve 12,12,12-trifluoro-8-dodecenoic acid (1.39g, 5.5 mmol) in ethanol (50 mL) and place in a Paar hydrogenation flask. Add 10% palladium/carbon (500 mg). Charge the vessel to 50 psi and shake for 18 hours. Filter through celite and remove the solvent in vacuo to give 12,12,12-trifluorododecanoic acid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05278171 |
| Source dataset | uspto-grants-1994_01 |
| ORD ID | ord-e9effd9104444fed90e67d06835ccbb4 |
| Source note | uspto-grants-1994_01 |