HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzene → N-(4-methoxyphenyl)-4-nitro-3-methylbenzene carboximidoyl chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzene | HCID 241 | — |
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | N-(4-methoxyphenyl)-3-methyl-4-nitrobenzamide | HCID 790964 | — |
| Product | N-(4-methoxyphenyl)-4-nitro-3-methylbenzene carboximidoyl chloride | HCID 13633435 | — |
Reaction Steps
14 g of N-(4-methoxyphenyl)-4-nitro-3-methyl benzamide in suspension in 70 ml of thionyl chloride were heated for 20 hours at reflux. The solvent was eliminated by entrainment with benzene, and after drying under reduced pressure at ambient temperature, 15 g of N-(4-methoxyphenyl)-4-nitro-3-methylbenzene carboximidoyl chloride melting towards 80° C. were obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05278180 |
| Source dataset | uspto-grants-1994_01 |
| ORD ID | ord-d6a32888520145e7b0f7ea42659d374a |
| Source note | uspto-grants-1994_01 |