HuagongsheHuagongshe Chemistry Print Report · For research reference only
o-Chloranil → 4-(7-Methoxynaphth-1-yl)-1-methylpiperidine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | o-Chloranil | HCID 73252 | — |
| Reactant | 4-(3,4-Dihydro-7-methoxynaphth 1-yl)-1-methylpiperidine | HCID 19096248 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 4-(7-Methoxynaphth-1-yl)-1-methylpiperidine | HCID 19105262 | — |
Reaction Steps
A mixture of 11.5 g of the product from Example 15 and 23.1 g of tetrachloro-1,2-benzoquinone in solution in 600 ml of anhydrous ethyl alcohol is refluxed for 30 hours.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05278185 |
| Source dataset | uspto-grants-1994_01 |
| ORD ID | ord-46f1fc549ba44a5b85ec5e110333bbe9 |
| Source note | uspto-grants-1994_01 |