Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Methyldichlorosilane → Silane, dichloro-5-hexen-1-ylmethyl-
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Methyldichlorosilane | HCID 6376 | — |
| 반응물 | 1,5-Hexadiene | HCID 11598 | — |
| 반응물 | 5-Hexenyldimethylchlorosilane | HCID 11829976 | — |
| 촉매 | Platinum | HCID 23939 | — |
| 생성물 | Silane, dichloro-5-hexen-1-ylmethyl- | HCID 11063373 | 68% |
반응 단계
Procedure is similar to the one described above for 5-hexenyldimethylchlorosilane. 8.4 g (100 mmole) of 1,5-Hexadiene was refluxed with platinum catalyst (100ppm). To the mixture 5.7 g (50 mmole) of methyldichlorosilane was added dropwise over 30 min. period. The completion of the reaction was monitored by infrared spectroscopy. The product distilling at 65° C./0.22 mm was obtained in 68% yield.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05278244 |
| 출처 데이터셋 | uspto-grants-1994_01 |
| ORD ID | ord-29bfa71d9dec400bb8337b4921eda113 |
| 출처 메모 | uspto-grants-1994_01 |