HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dichlorodimethylsilane → Indene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dichlorodimethylsilane | HCID 6398 | — |
| Reactant | HCID 17819667 | HCID 17819667 | — |
| Product | Indene | HCID 7219 | 16.7% |
Reaction Steps
3.9 g (22.7 mmol) of indene b4 were reacted with dimethyldichlorosilane and the mixture was worked up, analogously to instructions I.4. Column chromatography gave, in addition to 0.44 g of unused indene, 3.0 g of product b5 as a yellow oil (isomers). The yield as 65% with respect to Si and 73% with respect to the starting material reacted.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05278264 |
| Source dataset | uspto-grants-1994_01 |
| ORD ID | ord-0f7e19237f9b40508d8607690ac56cc6 |
| Source note | uspto-grants-1994_01 |