2-(Methylamino)ethanol → HCID 18959735, compound
Reaction equation
[OH:1][C:2]1[CH:3]=[C:4]2[C:9](=[CH:10][CH:11]=1)[O:8][C:7]([C:12]1[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=1)=[CH:6][C:5]2=[O:18].Br[CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][Cl:26].[OH:27][CH2:28][CH2:29][NH:30][CH3:31]>>[ClH:26].[OH:27][CH2:28][CH2:29][N:30]([CH3:31])[CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][O:1][C:2]1[CH:11]=[CH:10][C:9]2[O:8][C:7]([C:12]3[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=3)=[CH:6][C:5](=[O:18])[C:4]=2[CH:3]=1Participants
4
Procedure
The compound was prepared by a method similar to Example 1 from 6-hydroxyflavone, 1-bromo-6-chlorohexane, and 2-hydroxyethylmethylamine: mp 134°-137° C.
Sources & evidence
- ORD record
- ord-da6405491eb04f5aaf67fe7971dbab37
- Source dataset
- uspto-grants-1994_01
- Patent number
- US05278174
Reaction notes
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