Dimethylamine → HCID 14982952, compound
Reaction equation
[OH:1][C:2]1[CH:3]=[C:4]2[C:9](=[CH:10][CH:11]=1)[O:8][C:7]([C:12]1[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=1)=[CH:6][C:5]2=[O:18].Br[CH2:20][CH2:21][CH2:22][CH2:23][CH2:24]Cl.[CH3:26][NH:27][CH3:28]>>[CH3:26][N:27]([CH3:28])[CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][O:1][C:2]1[CH:11]=[CH:10][C:9]2[O:8][C:7]([C:12]3[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=3)=[CH:6][C:5](=[O:18])[C:4]=2[CH:3]=1Participants
4
Procedure
The compound was prepared by the method of Example 3 from 6-hydroxyflavone, 1-bromo-5-chloropentane, and dimethylamine: mp 82°-83 ° C.
Sources & evidence
- ORD record
- ord-63633c2abccd435b812af584a5314d3e
- Source dataset
- uspto-grants-1994_01
- Patent number
- US05278174
Reaction notes
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