HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,6-Diisopropylphenyl isocyanate → HCID 14969214, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,6-Diisopropylphenyl isocyanate | HCID 92259 | — |
| Reactant | Lithium diisopropylamide | HCID 2724682 | — |
| Reactant | HCID 14969213 | HCID 14969213 | — |
| Product | HCID 14969214 | HCID 14969214 | 100% |
Reaction Steps
The title compound was prepared from 13-[(tetrahydro-2H-pyran-2-yl)oxy]-2-tridecanone (2.0 g, 0.006 mol), 2,6-diisopropylphenyl isocyanate (1.36 g, 0.006 mol), and lithium diisopropylamide (0.006 mol) using the procedure described in Example 1. Purification by flash chromatography (silica gel, 10% EtOAc/hexane) yielded 3.11 g (0.006 mol, 93%) of the desired product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05278326 |
| Source dataset | uspto-grants-1994_01 |
| ORD ID | ord-80388194763f45d1883755d86dcf00f6 |
| Source note | uspto-grants-1994_01 |