HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tetradecan-2-one → HCID 10251296, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tetradecan-2-one | HCID 75364 | — |
| Reactant | 2,6-Diisopropylphenyl isocyanate | HCID 92259 | — |
| Reactant | Lithium diisopropylamide | HCID 2724682 | — |
| Product | HCID 10251296 | HCID 10251296 | 44% |
Reaction Steps
The title compound was prepared from 2-tetradecanone (5.0 g, 0.023 mol), 2,6-diisopropylphenylisocyanate (4.78 g, 0.023 mol), and lithium diisopropylamide (0.023 mol) using the procedure described in Example 1. Purification by flash chromatography (silica gel, 15% EtOAc/hexane) yielded 4.25 g (0.010 mol, 44%) of the desired product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05278326 |
| Source dataset | uspto-grants-1994_01 |
| ORD ID | ord-6c6a19d3c466406d94324dc27b26dc59 |
| Source note | uspto-grants-1994_01 |