HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-Methylaniline → HCID 67850484, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-Methylaniline | HCID 7515 | — |
| Reactant | HCID 10063724 | HCID 10063724 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 67850484 | HCID 67850484 | 85.5% |
Reaction Steps
2-(4-Methoxy-2-methylphenylamino)-4-chlorothieno[3,2-d]pyrimidine (4 g, 0.013 mol) and N-methylaniline (2.8 g, 0.026 mol) were heated at 140° for 1 hour. The addition of diethyl ether gave a solid which was collected by filtration and dried, (5.5 g). Recrystallization from ethanol/diethyl ether gave the title compound, (4.59 g), m.p. 225°-227°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05280026 |
| Source dataset | uspto-grants-1994_01 |
| ORD ID | ord-2570251ccb374a4aab5849ca0d0fff32 |
| Source note | uspto-grants-1994_01 |