反应详情

温度

100 °C

Diethyl malonate (1.76g, 0.011 moles), paraoctylbenzaldehyde (2.4g, 0.011 moles) and piperidine (5 drops) were heated to 98° C. for 2.5 hrs. and 45° C. for 16 hrs. The solution was heated to 100° C. for 64 hrs. The title compound was purified by silica gel chromatography. The structure assignment was supported by NMR, infrared and uv spectra and elemental analysis (360.5).

1. customThe title compound was purified by silica gel chromatography